Over the past half-decade, the functionalized Fe3O4 nanoparticles have been applied to organic synthesis as heterogeneous nanocatalysts. Due to the magnetic properties, the functionalized Fe3O4 nanoparticles have been preferred over other catalytic systems. In addition, the unique physical, chemical, and magnetic field properties of Fe3O4 nanoparticles have led to the development of them for efficient […]
Single-atom catalysts have recently received much scientific attraction as sustainable catalysts due to their greater activity and selectivity arising from the uniform distribution, electronic properties, and quantum mechanical interactions at the nanoscale of single atoms coupled with interactions at the metal-support interfaces. Carbon-based materials are an excellent support material for single-atom catalysts owing to their […]
Fe-doped TiO2 nanoparticles were successfully synthesized by the coprecipitation method. TiO2 was doped with a different molar ratio of iron amounts, namely 0.1% and 0.2%. An undoped TiO2 was also prepared for comparison. X-ray diffraction (XRD), transmission electron microscopy (TEM) and UV-visible diffuse reflectance spectroscopy techniques were used to characterize the as-synthesized nanoparticles. The XRD […]
In this investigation, a fluidized bed photocatalytic reaction system was designed to eliminate emerging contaminants: acetaminophen and pyridine in water. Titanium dioxide (TiO2) doped with aluminum (Al3+) using the photo-deposition technique was used as a catalyst and supported on alumina beads (Al2O3). The catalyst´s doping was carried out by photo deposition with aluminum particles. The […]
In this study, we discuss the wet chemical synthesis and experimental analysis of zinc doped Gd2O3(Gd2-xZnxO3-δ) nanoparticles where, x=0, 0.1, 0.2, 0.3, 0.4, and 0.5. The cubic crystalline structure is derived from XRD results and the existence of metal-oxide bond has been confirmed from FTIR studies. According to SEM and PSA analysis, the produced nanoparticles […]
We studied the reaction in which carbon monoxide is converted to hydrocarbons, and investigated the behaviors and the combination system of catalysts exchanged with platinum and ammonium ions. Experiments were conducted at 1.2 MPa, 523K, and CO/H2=1 ratio. The structure and the texture of the catalysts, assessed by XRD, BET/BJH, and SEM, exhibited a microporosity […]
In this study, the electrochemical determination of oxazepam in plasma samples was studied. The composite of graphene oxide/boron (B-RGO) was synthesized via the hydrothermal method and it was cast on the glassy carbon electrode (GCE). The polyaspartic acid (poly(ASP)) was deposited on the B-RGO by electropolymerization to prepare the modified electrode named B-RGO/ poly(ASP)|GCE. The […]
In this research work, Nano-SiO2/Taurine was synthesized and characterized by FT-IR, energy dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), X-ray diffraction patterns (XRD) ,Thermogravimetric analysis (TGA) and MAP analysis. Nano-SiO2/Taurine has considerable benefits such as simple preparation protocol, simple handling, high acidic property, reusability and high stability. Nano-SiO2/Taurine was used as a catalyst for […]
In this study, two different methods were described for the synthesis of 2-(aryl)-3-((2-oxo-2-(2-oxo-2H-chromen-3-yl)ethyl)amino)imidazolidin-4-one derivatives under microwave irradiation. The first method was step by step method. In step by step method, 3-(2-hydrazinylacetyl)-2H-chromen-2-one and aromatic aldehydes in 1 mL of absolute ethanol were irradiated with appropriate power within 3-10 min to obtain imine products. Then, the imine […]
Modification of sodium montmorillonite was conducted using zirconium phosphate. The effect of a series of phosphate precursors such as dihydrogen phosphate, diammonium hydrogen phosphate, and sodium phosphate was observed. The catalyst was used in the conversion of methanol dimethyl ether using 1 g of catalyst at a temperature range of 150-350 ˚C with a Liquid […]