An efficient four-component synthesis of benzopyranopyridines is described by one-pot condensation of salicylaldehydes, thiols and 2 equiv of malononitrile with nano-PbWO4 as a robust and reusableheterogeneous catalyst under ultrasonic irradiation. Lead tungstate (PbWO4) nanostructures have been synthesized via a sonochemical method based on the reaction between lead (II) nitrate and sodium tungstate dihydrate in an […]
In this study, a novel and environmentally benign o-phenylendiamine stabilized on silica-coated Fe3O4 magnetic nanocatalyst (Fe3O4@SiO2@propyltriethoxysilane@o-phenylendiamine-SO3H/HCl) as a hybrid magnetic organometallic nanocatalyst has been synthesized. After that, the structure of this new catalyst was completely characterized via Fourier transforms infrared (FT-IR) spectroscopy, Brunauer–Emmett–Teller (BET), atomic force microscopy (AFM), field-emission scanning electron microscopy (FE-SEM) images, energy […]
A proper, atom-economical, straightforward one-pot multicomponent synthetic route for the synthesis of benzopyranophenazines has been presented by the reaction of hydroxynaphthoquinone, o-phenylenediamine, benzaldehydes, and malononitrile with crosslinked sulfonated polyacrylamide (Cross-PAA-SO3H) attached to nano-Fe3O4as an efficient heterogeneous solid acid catalyst under ultrasonic irradiations in ethanol. Experimental simplicity, wide range of products, excellent yields in short reaction […]
