A facile chemical mixing approach was used to prepare TiO2/ZnO photocatalystswith different mass ratios. The photodegradation activity was tested against paracetamol in an aqueous phase assisted by low UVC-light intensity (9 W). TiO2/ZnO particles mainly exhibited irregular shapes with uniform distributions and high crystallinity degree, the primary oxidation state in the structure is titanium […]
Immobilization of catalysts on the surface of some inert supports makes therecovering step easier. Because of the specific physicochemical properties, zeolites are good candidate as catalyst supports. In this study, zeolite X was synthesized by natural kaolin and TiO2 was incorporated into zeolite phase by impregnation method. Degradation of Safranin Orange, methylene blue and 2,4–dinitroaniline […]
In this paper CuFe2O4, nanocrystalline powders were prepared. Also, the supported Cu ferrite was obtained by impregnation of the supports with Cu and Fe nitrates solutions, for calcination temperature 450 ºC. The samples were characterized by X-ray powder diffraction (XRD) and Fourier transform-infrared spectroscopy (FT-IR). Photocatalytic degradation of acid red 206 in water was studied. […]
Taguchi experimental design technique was used for optimization of photodegradation of yellow water sample of trinitrotoluene (TNT) production process. The nanoparticles of doped N-TiO2 were also used as photocatalysts in the photodegradation reaction under visible light. The ranking of data based on signal to noise ratio values showed that the importance order of the factors […]
In this study, iron nanoparticles (FeNPs) were synthesized by green route under microwave irradiation. Terminalia arjuna bark extract was used for synthesis, which acts as reducing and stabilizing agent. The synthesized FeNPs were characterised by UV-Visible spectra, X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectra (FT-IR), BET surface area and UV-DRS (diffuse […]
Novel metal oxides have been studied worldwide due to their potential uses in ecological refinement, particularly to eliminate organic impurities present in water. In this work, we report the preparation of Ni1-xCoxAl2O4-δ (where x=0, 0.05, 0.10, 0.15 and 0.20) nanoparticles by simple chemical precipitation route. The as-synthesized spinel particles were characterized by X-ray diffraction (XRD), […]
Here, SnO2, BiVO4, and CuO nanoparticles (NPs) were hydrothermally synthesized and mixed in an agate mortar mechanically. The coupled ternary SnO2-BiVO4-CuO (SBC) catalyst and the individual NPs were then briefly characterized by powder X-ray diffraction (XRD), scanning electron microscope (SEM), and diffuse reflectance spectroscopy (DRS). Average crystallite size of 25 nm was obtained from the […]
In this work, ZrO2/TiO2/ZnO ternary nanocomposites were prepared by the sol-gel technique. The Taguchi method with the L9 orthogonal array was utilized to optimize the experimental conditions for the preparation of nanocomposites. The design has four factors, and each factor has three levels. The design factors of this study were calcination temperature, the aging time, […]
Zinc Oxide nanoparticles (ZnONPs), which have well-known antimicrobial properties, are used extensively in various medical and general applications. In this analysis, 70-gram positive bacterial isolates were obtained from 100 patients using cardiac catheterization, with 54 Staphylococcus aureus and 16 other positive pathogenic bacteria. Accordingly, morphological, cultural and biochemical testes confirmed the results by VITEK 2 […]
In this investigation, a fluidized bed photocatalytic reaction system was designed to eliminate emerging contaminants: acetaminophen and pyridine in water. Titanium dioxide (TiO2) doped with aluminum (Al3+) using the photo-deposition technique was used as a catalyst and supported on alumina beads (Al2O3). The catalyst´s doping was carried out by photo deposition with aluminum particles. The […]