The aim of the present study was to prepare nano-sized calcium fluoride (CaF2). Calcium fluoride nanoparticles were synthesized by CaCl2.6H2O and ammonium fluoride. Nanoparticles were synthesized by co-precipitation method. The synthesized nanocrystals were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM). The crystallite size estimated using Scherer’s formula was […]
We have used Lithium Aluminum Hydroxide reducing method of silver nitrate to prepare heterogeneous silver-silica nanocomposite particles with thiol and amino groups serving to bind the Ag nanoparticles to the surfaces of the SiO2 nanoparticles. We examined products of these reductions using FTIR, SEM, XRD and UV-vis. spectroscopy. The SiO2 nanoparticles had diameters ranging from […]
Calcium fluoride nanoparticles with special amount of cerium ion (%1) were synthesized by coprecipitation. Fourier transforms infrared spectroscopy (FTIR), X-ray diffraction (XRD), absorption and photoluminescence (PL) from CaF2Ce nanoparticles has been investigated. FTIR spectra reveal that there are some amounts of OH, NO3 and other organic functional groups on the particle surfaces before the post […]
A new mixed halo chromate nanoparticle compound was synthesised and characterized. Triphenylphosphonium trifluoroiodochromate (III)[P(C6H5)3H]+[CrF3I]– nanoparticle was synthesized by using triphenylphosphonium iodide reaction with CrF3, in the presence of 3-mercaptopropionic acid. This method is a simple and direct method. The product was characterized by spectroscopic and analytical methods such as 31P-NMR, FT-IR, XRD, SEM. Theoretical calculations […]
Synthesis, characterization, spectral and theoretical calculations of sodium tetrafluoroborate (III) (STFB) has been studied in this research. Sodium tetrafluoroborate (III) was synthesized by a sonochemical method and characterized by IR, UV/VIS, 11B-NMR and Mass spectrometer techniques. The nano compound was characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRD) and IR spectroscopy. The structure […]
Synthesis, identification and thermal behavior studies of nanoparticles cobalt (II) bromide has been studied in this research. Cobalt (II) bromide was synthesized by planetary high-energy ball mill. The general formula of this compound is CoBr2.6H2O. The synthesized nanoparticles were characterized by Fourier transform infrared spectroscopy and also Size and structure of synthesized nanoparticles were studied […]
In this work, sol-gel processing was used to synthesize the fluorohydroxyapatite (nano-FHA, Ca10(PO4)6(OH)2−xFx) nanopowders. The advantages of the sol-gel method over other methods are precise control of composition, low processing temperature, and better homogeneity. Calcium nitrate tetrahydrate, phosphorous pentoxide and Tetrabuthylammonium fluoride were used, respectively, as P, Ca, and F precursors with a Ca:P ratio […]
