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Keyword: Nano silica chromic acid

Original Article
Nano silica chromic acid/wet SiO2 and NaNO2 as an efficient reagent system for synthesis of azo dyes based on 1-naphthol at room temperature and solvent-free conditions

A convenient, rapid, and one-pot method for the synthesis of azo dyes has been developed. In this protocol, diazotization reagent (ArN2+ -CrO3–SiO2) was prepared via grinding of aromatic amines, NaNO2, wet SiO2 and nano silica chromic acid (Nano-SCA) without solvent at room temperature. The obtained diazotization reagent was sufficiently stable to be kept at room […]