Fe3O4-containing cotton-like mesoporous silica system (Fe3O4@NCSM) was studied with regard to its performance towards the photodecolorization of bromothymol blue (BTB) aqueous solution. The surface properties of the functionalized catalyst were analyzed by a series of characterization techniques like FTIR, XRD, BET, SEM and TEM. The N2 Adsorption–desorption analysis shows that the mesostructure of silica remains […]
The surface ofFe3O4 magnetic nanoparticles (MNPs) was modified by L-cysteine through condensation of COOH groups of L-cysteine and OH groups on the surface of Fe3O4. The –SH group of preparedFe3O4@Cys MNPs oxidized to –SO3H group and Fe3O4@Cys–SO3H as an environmentally friendly magnetic nanoparticle was prepared. The MNPs were characterized by FT-IR, XRD, SEM and TEM […]
A three-component process for the one-pot synthesis of 6-amino-4-aryl-5-cyano-3-methyl-1-phenyl-1,4-dihydropyrano[2,3-c]pyrazoles is described by the three-component reaction of aldehydes, 3-methyl-1-phenyl-1H-pyrazol-5(4H)-one and malononitrile in the presence of Fe3O4@FSM-16-SO3H as an efficient magnetically recyclable mesoporous catalyst. Folded sheet mesoporous material (FSM-16) was prepared by intercalation of a layered, kanemite type sodium silicate with cetyltrimethylammonium (CTMA) ions in the presence […]
Fe is an important element, used in soft magnetic materials (cores) in electrical and electronic devices and its concentration in e-waste is high. Thus, this study is aimed to recover Fe from the soft magnetic FeSiAl cores of spent printed circuit boards (PCBs). Here, the Fe-rich FeSiAl cores were identified, separated manually, and subjected to […]