Cobalt vanadate (Co3V2O8) nanoparticles were prepared by a hydrothermal process using ammonia metavanadate and cobalt nitrate as precursors and calcined at 450 °C to obtain pure Co3V2O8 nanoparticles. The sample was characterized by scanning electron microscopy, X-ray diffraction, Fourier transform infrared, and UV-visible diffuse reflectance spectroscopy. The characterization analysis confirmed variations in the structure, shape, […]
ZrO2 nanopowder was prepared by the sol-gel auto-combustion method. The product was characterized by X-ray diffraction (XRD), energy dispersive analysis of X-ray (EDX) and scanning electron microscopy (SEM). The average crystalline size of ZrO2 was obtained 62 nm. Also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale ZrO2 under UV light irradiation was […]
ZnO and ZrO2 photo catalysts were synthesized by sol-gel auto combustion method. The products were characterized by X-ray Diffraction (XRD) and Scanning Electron Microscopy (SEM). Structural and morphological properties of nano particles were investigated and the average crystalline size of ZnO and ZrO2 was obtained 44 and 51 nm, respectively. Also, photo catalytic degradation of […]
ZnO and Mn-ZnO nano powders were prepared by the sol-gel auto combustion method. The products were characterized by X-ray diffraction (XRD), energy dispersive analysis of X-ray (EDX) and scanning electron microscopy (SEM). Structural and morphological properties of nano particles were investigated and the average crystalline size of ZnO and Mn-doped ZnO was obtained 44 and […]
The present work is focused on the degradation of 4-chloro-2-nitrophenol in aqueous solution containing nano titanium dioxide, hydrogen peroxide and the combination of nano-TiO2/H2O2. The effect of experimental parameters, such as the amount of nano- TiO2 concentration of H2O2, initial concentration of 4-chloro-2-nitrophenol and pH on the reaction was investigated. Experimental data […]
This paper reports the synthesis and characterization of photocatalyst CdS nanoparticles for investigation of photocatalytic degradation of 2,4,6-trichlorophenol. CdS nanoparticles were synthesized by the microwave-assisted sol-gel method and characterized by various techniques such as X-ray diffraction, filed emission scanning electron microscopy, energy dispersive spectroscopy, Fourier transform infrared spectroscopy and UV-visible spectrophotometer. The average crystallite size […]
ABSTRACT: In this project, a nano catalyst (TiO2) and ozone combined with each other and they were used for the removal of 4-nitrophenol (4NP) in industerial wastewater. The effect of some operational parameters such as initial pH (3-9), the concentration of pollutant (20-80 mg/L), and amount of TiO2 were investigated. In O3/TiO2 process, the anion […]
Template synthesis is a powerful method for the preparation of nanoscale materials with specific size and shape. Cadmium oxide (CdO) nanoparticles were synthesized by using sodium dodecyl sulfate (SDS), Cd(OAc)2.2H2O and sodium hydroxide as starting materials. The sample was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM). The XRD pattern proves that the final […]
ZnO- nanoparticles with an average particle size of 24 nm were successfully synthesized using the microwave assisted sol- gel technique. Structural and morphological properties of the nanoparticles were characterized by X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM), Energy disperse spectrum (EDS) and Fourier transform infrared spectroscopy (FTIR). The band gap energy was measured […]
