ZnO thin films with preferred orientation along the (002) plane were prepared onto the glass substrates by the sol-gel spin coating method for different post- annealing temperatures. The XRD study confirms that the thin films grown by this method have good crystalline hexagonal wurtzite structure. The optical band gap of the samples was determined from […]
ZnO nanorod was prepared by microwave assisted method. The crystal structure of the nano powders were confirmed by X-Ray diffraction analysis and the mean particle size was estimated by the Scherrer,s formula .The surface morphology of the nano particles were analyzed by using SEM . The absorption spectrum of the material in the UV-Vis range […]
Two-component reaction of 2-aminobenzophenones with acetylenic esters in the presence of γ-Al2O3 and Cu/ZnO as suitable heterogeneous catalysts has been studied. Nano γ-Al2O3 and Cu/ZnO showed high activities when used as surface catalysts for the synthesis of quinoline derivatives. After completion of the reaction, the catalyst was recovered and reused several times under the same […]
A new three-dimensional unit cell model has been developed for modeling three constituent phases including inclusion, interphase and matrix. The total elastic modulus of nano-composite is evaluated. Numerical results are in good agreement with the previous proposed theoretical modeling. Higher matrix and inclusion elastic modulus both can dramatically influence the total elastic modulus.
ZnO and ZrO2 photo catalysts were synthesized by sol-gel auto combustion method. The products were characterized by X-ray Diffraction (XRD) and Scanning Electron Microscopy (SEM). Structural and morphological properties of nano particles were investigated and the average crystalline size of ZnO and ZrO2 was obtained 44 and 51 nm, respectively. Also, photo catalytic degradation of […]
Ceramic Ultrafiltration membranes are considered as an alternative for the treatment of both stable water-in-oil and oil-in-water emulsions proved to be more effective in comparison with other conventional techniques. In this study, symmetric macro-porous ceramic membranes are prepared through dry pressing of α-alumina powder and the addition of various binders including Poly (vinyl alcohol). The […]
In this study the effect of using multi-walled carbon nanotube (MWCNT) on flexural and compressive strengths, ultimate displacement and energy absorption capability of standard cement mortar considering different weight percentages of nanotubes as well as different dispersion methods has been investigated. Influential point in adding nanotubes to the composites is their proper dispersion, which is […]
A novel complex of cadmium (II) [CdL0.5(NO3)(H2O)](1), L= N,N-bis (O-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. Compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by IR, 1HNMR spectroscopy, X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The gray single crystal of compound 1 […]
Porous silicon samples were prepared by electrochemical etching method for different etching times. The structural properties of porous silicon (PS) samples were determined from the Atomic Force Microscopy (AFM) measurements. The surface mean root square roughness (σ rms) changes as function of porosity were studied, and the influence of etching time on porosity and roughness […]
Polyimide/Nickel oxide (polyimide/NiO) nanocomposite was successfully synthesized by sol gel technique, using Pyromellitic dianhydriede (PMDA), 4,4-oxydianiline (ODA) and N,N-dimethylacetamide (DMAC) and 10 wt% Nickel titanate nanopowders (NPs). Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM) were used to characterize the structure and properties of the obtained […]