Nanostructured Ni2As2O7 semiconductor samples were synthesized by a solid state method among As2O3 and Ni(NO3)2.6H2O raw materials at 650 °C (S1) and 750 °C (S2) as reaction temperatures. The synthesized nanomaterials were characterized by powder X-ray diffraction (PXRD) technique and Fourier-transform infrared (FTIR) spectroscopy. The Rietveld analysis showed that the obtained materials were crystallized well […]
Nanostructured Ni1-xLnxSb2O6 (Ln = Eu, Gd, Ho and Yb) powders were synthesized via stoichiometric 1:2 Ni:Sb molar ratio by solid state reaction at 800 ºC for 8 h using Ni(NO3)2, Sb2O3, Eu2O3, Gd2O3 and Ho2O3 raw materials. The synthesized materials were characterized by X-ray diffraction (XRD) technique. Structural analyses were done by FullProf program employing […]