Published in Issue 2014-11-01
How to Cite
Akhoon, S. A., Rubab, S., & Shah, M. A. (2014). A benign hydrothermal synthesis of nanopencils-like zinc oxide nanoflowers. International Nano Letters, 5(1 (March 2015). https://doi.org/10.1007/s40089-014-0130-7
HTML views: 54
PDF views: 102
Abstract
Abstract Synthesis of zinc oxide (ZnO) nanoflowers and nanopencils is normally carried out with the help of structure-directing chemicals and templates. Besides releasing environmentally toxic substances, the use of these chemicals restricts the practical applications of nanostructures. In this paper, we report a typical template-free and environmentally benign synthesis of ZnO nanoflowers with nanopencils-like petals through a facile hydrothermal method. The as-synthesized ZnO nanoflowers were characterized using X-ray diffraction, field emission scanning electron microscopy, tunneling electron microscopy (TEM), high resolution TEM, and energy-dispersive X-ray spectroscopy techniques. The results reveal high quality and impurity-free hexagonal wurtzite phase ZnO nanoflowers of nanopencils-like petals having a length of 100–150 nm and a diameter of 45–60 nm.Keywords
- Hydrothermal,
- Environmentally benign,
- Nanoflower,
- Nanopencils,
- Economical
References
- Lazoryak et al. (2003) Ferroelectric and ionic-conductive properties of nonlinear-optical vanadate, Ca9Bi(VO4)7 (pp. 3003-3010) https://doi.org/10.1021/cm031043s
- Felix et al. (2004) Biofunctionalization of fluorescent rare-earth-doped lanthanum phosphate colloidal nanoparticles (pp. 5954-5957) https://doi.org/10.1002/anie.200460856
- Tretyakov, Y.D. (ed.): Nanotechnologies. The alphabet for everyone. Fizmatlit, pp. 344–345 (2008)
- Al-Harbi et al. (2011) Growth of ZnO nanorods and their optical properties (pp. 87-91)
- Ebrahim, S., Khanlari, M.R., Durani, R.S.: Study of ZnO nanopencils and nanoneedles morphology synthesized on quartz substrate in ambient air and without catalyst. In:4th International Conference on Nanostructures (ICNS4). pp. 679–680 (2012)
- Jiang et al. (2007) Improved dye sensitized solar cells with a ZnO nanoflower photoanode https://doi.org/10.1063/1.2751588
- Hsueh and Hsu (2008) Fabrication of gas sensing devices with ZnO nanostructures by the low temperature oxidation of zinc particles (pp. 572-576) https://doi.org/10.1016/j.snb.2007.12.045
- Ge et al. (2008) Preparation and gas sensing property of ZnO nanorod bundle thin films (pp. 2307-2310) https://doi.org/10.1016/j.matlet.2007.11.073
- Kharisov (2008) A review for synthesis of nanoflowers (pp. 190-200) https://doi.org/10.2174/187221008786369651
- Moulani and Sediri (2013) Pencil-like zinc oxide micro/nano-scale structures: hydrothermal synthesis, optical and photocatalytic properties (pp. 3723-3728) https://doi.org/10.1016/j.materresbull.2013.05.116
- Badgujar et al. (2014) A simple protocol for synthesis of pencil-like ZnO rods and their photocatalytic performance study (pp. 1-6) https://doi.org/10.1166/jnan.2014.1172
- Tan et al. (2014) Growth of waist ZnO twin rods through hydrothermal synthesis (pp. 3233-3238) https://doi.org/10.1166/jnn.2014.8595
- Baruah and Dutta (2009) Hydrothermal growth of ZnO nanostructures https://doi.org/10.1088/1468-6996/10/1/013001
- Al-Hartomy and Shah (2011) Safe and simple approach to prepare hexagonal ZnO nanostructures in water (pp. 139-142)
- Shah et al. (2009) Simple approach for the synthesis of zinc oxide nanorods (pp. 66-73) https://doi.org/10.1504/IJNP.2009.028738
- Sofi and Shah (2014) The study of structural and morphology features of indium oxide nanostructures https://doi.org/10.1088/2053-1591/1/1/015041
- Wang and Yang (2005) Thermodynamics of metastable phase nucleation at the nanoscale (pp. 157-202) https://doi.org/10.1016/j.mser.2005.06.002
- Pol et al. (2008) Facile synthesis of novel photoluminescent ZnO micro- and nanopencils https://doi.org/10.1021/la803008g
- Yu et al. (2011) Hydrothermal synthesis and characterization of ZnO films with different nanostructures (pp. 5563-5565) https://doi.org/10.1016/j.apsusc.2011.01.039
- Wu and Liu (2002) Catalyst-free growth and characterization of ZnO nanorods (pp. 9546-9551) https://doi.org/10.1021/jp025969j
- Suhaimi et al. (2014) A catalyst-free growth of aluminum-doped ZnO nanorods by thermal evaporation (pp. 256-265) https://doi.org/10.1186/1556-276X-9-256
10.1007/s40089-014-0130-7