OICC Press Journal of Nanostructure in Chemistry 2193-8865 4 2 (June 2014) 2014 04 23 Electrochemical detection of l-serine and l-phenylalanine at bamboo charcoal–carbon nanosphere electrode 10.1007/s40097-014-0102-5 EN Mitali Saha Department of Chemistry, National Institute of Technology, Agartala, Tripura, 799055, IN Soma Das Department of Chemistry, National Institute of Technology, Agartala, Tripura, 799055, IN Journal Article 2014 04 23 Abstract A carbon nanosphere electrode (CN) has been fabricated for the electrochemical detection of l -serine and l -phenylalanine. Electrochemical behavior of amino acids was investigated using cyclic voltammetry, differential pulse voltammetry, square wave voltammetry and linear sweep voltammetry. In optimal conditions, the peak current of both amino acids on the CN electrode was found to enhance greatly. A sensitive oxidation peak at 0.085 V was observed in the determination of l -serine and 0.06 V for l -phenylalanine. A linearity between the oxidation peak current and the concentration of both amino acids was obtained in the range of 1–100 µM ( R 2  = 0.99783 for l -serine, 0.99618 for l -phenylalanine). The practical application of the carbon nanosphere electrode in the determination of the amino acids possesses high selectivity, sensitivity and stability.