TY - EJOUR
AU - Ghane, M.
AU - Sadeghi, B.
AU - Jafari, A.R.
AU - Paknejhad, A.R.
PY - 2024
DA - March
TI - Synthesis and characterization of a Bi-Oxide nanoparticle ZnO/CuO by thermal decomposition of oxalate precursor method
T2 - International Journal of Nano Dimension (Int. J. Nano Dimens.)
VL - 1
L1 - https://oiccpress.com/international-journal-of-nano-dimension/article/synthesis-and-characterization-of-a-bi-oxide-nanoparticle-zno-cuo-by-thermal-decomposition-of-oxalate-precursor-method/
DO - 10.7508/ijnd.2010.0x.003
N2 - In the present work, we report the synthesis of binary nano metal oxides such as Zinc /Copper Oxide via novel dry synthetic methods such as thermal decomposition of oxalate precursor. The synthesis route involves facile solid-phase mechanochemical activation of a physical mixture of simple copper/zinc salts and oxalic acid, followed by calcination of the as-ground oxalate precursors at 450◦C. X-ray powder diffractometry (XRD), infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) were used to the thermal spectroscopic, structural, morphological characterization and surface area determination of the product respectively . An average nanocrystallite size of 5.0 nm was obtained for Zn/Cu, as estimated by the Scherrer’s equation.
IS - 1
PB - OICC Press
KW - Nanoparticle, Chemical synthesis, Bi-Oxide, Zinc / Copper oxide, Thermal Decomposition of Oxalate Precursor Method 
EN -