TY - EJOUR AU - Ranjbar, Z. Rashidi AU - Sheikhshoaie, I. AU - Bagheri, Z. PY - 2024 DA - February TI - Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet T2 - International Journal of Nano Dimension (Int. J. Nano Dimens.) VL - 5 L1 - https://oiccpress.com/international-journal-of-nano-dimension/article/solid-state-preparation-of-cdo-nano-particles-by-thermolysis-of-a-precursor-as-compacted-nanosheet/ DO - 10.7508/ijnd.2014.04.013 N2 - A novel complex of cadmium (II) [CdL0.5(NO3)(H2O)](1), L= N,N-bis (O-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. Compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by IR, 1HNMR spectroscopy, X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The gray single crystal of compound 1 has been synthesized by slow evaporation and characterized by IR, 1HNMR spectroscopy. Then, Compound 1 in nano size was used as initial reagent to obtain nano-particles of cadmium (II) oxide at 673 K by direct calcination. The obtained CdO nano-particles were characterized by XRD pattern as well as SEM images. IS - 4 PB - OICC Press KW - Nanoparticle, CdO, Sonochemistry, Cadmium (II) complex, Thermolysis EN -