TY - EJOUR AU - Darzi, S. Janitabar AU - Mahjoub, A. R. AU - Bayat, A. PY - 2024 DA - February TI - Synthesis and characterization of visible light active S-doped TiO2 nanophotocatalyst T2 - International Journal of Nano Dimension (Int. J. Nano Dimens.) VL - 7 L1 - https://oiccpress.com/international-journal-of-nano-dimension/article/synthesis-and-characterization-of-visible-light-active-s-doped-tio2-nanophotocatalyst/ DO - 10.7508/ijnd.2016.01.004 N2 - S-doped and bare mesoporous TiO2 were prepared using titanium tetraisopropoxide and thiocarbamide as raw materials. Prepared materials were characterized by means of fourier transform infrared spectroscopy FT-IR, thermogravimetry-differential scanning calorimetry (TG-DSC), X-ray diffraction (XRD), UV–Vis absorption spectroscopy, Brunauer–Emmett–Teller (BET) specific surface area and Barrett–Joyner–Halenda (BJH) pore size distribution analyses, scanning electron microscopy (SEM) and Energy-dispersive X-ray spectroscopy (EDX). The band gap of S-doped was estimated from UV-Vis spectroscopy data to be 2.8 eV. The specific surface area of S-doped TiO2 nanoparticles obtained via the BET method, calculated to be 181.3 m2/g and its pore size distribution curve revealed that the average diameter of the pores is 12.3 nm using BJH method. Photocatalytic efficiency of synthesized S-doped mesoporous TiO2 was tested for degradation of Congored azo dye under ultraviolet and visible lights. The results revealed that the S-doped mesoporous TiO2 is the most effective under visible light in comparison with bare one. IS - 1 PB - OICC Press KW - Band gap, Congored, S-doped TiO2, Photocatalyst, Mesoporous EN -