OICC Press International Journal of Industrial Chemistry 2228-5547 15 2 2024 07 30 Synthesis of photocatalytic material based on polyaniline supported PVC/NiAl2O3/AlF3 nanocomposite 10.57647/j.ijic.2024.1502.16 EN Ilnaz Ahmadian Department of Chemistry, Islamic Azad University, North Tehran Branch, Tehran, Iran Maryam Kargar Razi Department of Chemistry, Islamic Azad University, North Tehran Branch, Tehran, Iran 0000-0001-5788-9849 Babak Sadeghi Department of Chemistry, Islamic Azad University, Tonekabon Branch, Tonekabon, Iran 0000-0003-0933-5782 Mahbobeh Nakhaei Department of Chemistry, Islamic Azad University, North Tehran Branch, Tehran, Iran Journal Article 2024 07 30 In this research, photocatalysis single AlF3, Ternary PVC/Al2O3/AlF3 (PNA) and polyaniline (PAI) supported PNA nanocomposite were synthesized by co-precipitation method. Surface area and morphological structure of the synthesized photocatalysts were characterized by X-ray Diffractometer (XRD), Brunauer-Emmett-Teller (BET), and Scanning Electron Microscopy (SEM). With the best conditions, the response in the glassy carbon electrode (GCE) showed concentrations of the malathion in the range values of 1.5-11 ×10−7 M, high recovery values around 98.4% with the good reproducibility. The stunning simplicity for preparation, and selectivity of this nanostructure and high sensitivity of polyaniline supported PNA electrode can make it a good candidate for application in detection of malathion.